Difference between revisions of "Preparation of coumaryl alcohol"
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This is a continuation of a [http://esr.monmsci.net/wiki/index.php/Synthesis_of_Lignin_Monomers#Introduction project] started in 2018 by [http://esr.monmsci.net/wiki/index.php/Alexandria_N_Tibbs A. Tibbs.] | This is a continuation of a [http://esr.monmsci.net/wiki/index.php/Synthesis_of_Lignin_Monomers#Introduction project] started in 2018 by [http://esr.monmsci.net/wiki/index.php/Alexandria_N_Tibbs A. Tibbs.] | ||
| − | [https://pubchem.ncbi.nlm.nih.gov/compound/p-Coumaryl-alcohol Coumaryl alcohol] will be synthesized from [https://pubchem.ncbi.nlm.nih.gov/compound/637542#section=Structures coumaric acid] through two separate reactions: | + | [https://pubchem.ncbi.nlm.nih.gov/compound/p-Coumaryl-alcohol Coumaryl alcohol] |
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| + | Coumaryl alcohol will be synthesized from [https://pubchem.ncbi.nlm.nih.gov/compound/637542#section=Structures coumaric acid] through two separate reactions: | ||
# First, coumaric acid will be converted into ethyl coumarate by through esterification. This will involve converting the carboxylic acid group into an ethyl ester group. | # First, coumaric acid will be converted into ethyl coumarate by through esterification. This will involve converting the carboxylic acid group into an ethyl ester group. | ||
# Finally, ethyl coumarate will be converted into coumaryl alcohol through a reduction reaction. | # Finally, ethyl coumarate will be converted into coumaryl alcohol through a reduction reaction. | ||
The experiment performed is based off of a [https://pubs.acs.org/doi/10.1021/jf506221p published paper] in which the authors previously synthesized coumaryl alcohol. The "Synthesis of p-Coumaryl Alcohol" subheading is what's important. | The experiment performed is based off of a [https://pubs.acs.org/doi/10.1021/jf506221p published paper] in which the authors previously synthesized coumaryl alcohol. The "Synthesis of p-Coumaryl Alcohol" subheading is what's important. | ||
Revision as of 05:07, 13 October 2021
Joseph Sampson, 10/21/21
This is a continuation of a project started in 2018 by A. Tibbs.
Coumaryl alcohol will be synthesized from coumaric acid through two separate reactions:
- First, coumaric acid will be converted into ethyl coumarate by through esterification. This will involve converting the carboxylic acid group into an ethyl ester group.
- Finally, ethyl coumarate will be converted into coumaryl alcohol through a reduction reaction.
The experiment performed is based off of a published paper in which the authors previously synthesized coumaryl alcohol. The "Synthesis of p-Coumaryl Alcohol" subheading is what's important.