MC Chem Wiki - User contributions [en]

Cryptocyanine

2017-02-09T22:59:17Z

BroddieD16:

Cryptocyanine

2017-02-09T22:58:39Z

BroddieD16:

Cryptocyanine

2017-02-09T22:54:13Z

BroddieD16:

Cryptocyanine

2017-02-09T22:52:44Z

BroddieD16:

File:UV-VisCryptocyanine.jpg

2017-02-09T22:50:10Z

BroddieD16: UV-Vis Spectra of Cryptocyanine. Wavelength was 648nm

UV-Vis Spectra of Cryptocyanine.
Wavelength was 648nm

File:CryptocyanineStructure.png

2017-02-09T22:48:45Z

BroddieD16: Structure of Cryptocyanine

Structure of Cryptocyanine

Cryptocyanine

2017-02-09T22:47:24Z

BroddieD16: Created page with "By Broddie Davis http://www.sigmaaldrich.com/catalog/product/aldrich/d91535?lang=en&region=US"

By Broddie Davis
http://www.sigmaaldrich.com/catalog/product/aldrich/d91535?lang=en&region=US

Emission Spectra of Different Metals

2017-02-02T03:32:43Z

BroddieD16:

[[Light_lab_Pchem|Return to Light lab]]

The instrument used for this experiment was the Ocean Optics Red Tide USB650 UV. Three metals were chosen for the experiment: Magnesium, Strontium, and Calcium. A magnesium ribbon, strontium, and calcium bits were used. The metals emission spectra were found by taking a piece of the metal and heating it up with a hand-held torch. First, the torch would heat the metal until the metal sparked. Once sparked it would emit a light. The length of emission of the light would depend on the metal and the amount. Once the metal emitted light, the distance from the metal to the detector had to be adjusted to get within a reasonable intensity.

[[File:Layout0.jpg|720px|thumb|left|Emission spectra of Magnesium Ribbon]]
[[File:Strontium.jpg|720px|thumb|left|Emission spectra of Strontium]]
[[File:Calcium.jpg|720px|thumb|left|Emission spectra of Calcium]]

File:Calcium.jpg

2017-02-02T03:31:03Z

BroddieD16: Calcium emission spectra

Calcium emission spectra

File:Strontium.jpg

2017-02-02T03:30:35Z

BroddieD16: Strontium emission spectra

Strontium emission spectra

Emission Spectra of Different Metals

2017-01-27T00:05:19Z

BroddieD16:

The instrument used for this experiment was the Ocean Optics Red Tide USB650 UV. Three metals were chosen for the experiment: Magnesium, Strontium, and Calcium. A magnesium ribbon, strontium, and calcium bits were used. The metals emission spectra were found by taking a piece of the metal and heating it up with a hand-held torch. First, the torch would heat the metal until the metal sparked. Once sparked it would emit a light. The length of emission of the light would depend on the metal and the amount. Once the metal emitted light, the distance from the metal to the detector had to be adjusted to get within a reasonable intensity.

[[File:Layout0.jpg|720px|thumb|left|Emission spectra of Magnesium Ribbon]]

Emission Spectra of Different Metals

2017-01-27T00:04:53Z

BroddieD16:

File:Layout0.jpg

2017-01-27T00:04:13Z

BroddieD16:

Emission Spectra of Different Metals

2017-01-26T23:59:12Z

BroddieD16:

The instrument used for this experiment was the Ocean Optics Red Tide USB650 UV. Three metals were chosen for the experiment: Magnesium, Strontium, and Calcium. A magnesium ribbon, strontium, and calcium bits were used. The metals emission spectra were found by taking a piece of the metal and heating it up with a hand-held torch. First, the torch would heat the metal until the metal sparked. Once sparked it would emit a light. The length of emission of the light would depend on the metal and the amount. Once the metal emitted light, the distance from the metal to the detector had to be adjusted to get within a reasonable intensity.

[[File:Magnesium.jpg|720px|thumb|left|Emission spectra of the laser cutter in use]]

File:Magnesium.jpg

2017-01-26T23:58:08Z

BroddieD16: Magnesium emission spectra

Magnesium emission spectra

Emission Spectra of Different Metals

2017-01-26T23:26:46Z

BroddieD16: Created page with "Three metals were chosen for the experiment: Magnesium, Strontium, and Calcium A magnesium ribbon was used, then strontium and calcium bits were used. The metals emission spec..."

Three metals were chosen for the experiment: Magnesium, Strontium, and Calcium A magnesium ribbon was used, then strontium and calcium bits were used. The metals emission spectra were found by taking a piece of the metal and heating it up with a hand-held torch. First, the torch would heat the metal until the metal sparked. Once sparked it would emit a light. The length of emission of the light would depend on the metal and the amount. Once the metal emitted light, the distance The instrument used for this experiment was the Ocean Optics Red Tide USB650 UV.

Broddie Davis Chem430 S17

2017-01-26T23:15:36Z

BroddieD16: Created page with "Chemistry Research 430 :Spring 2017 :Broddie Davis :Junior Chemistry Major ==Research Times== M/Tues 1-5 pm W 12:30-2 : section 02 = 0.50 credit = 8 hours per week. ==Propo..."

Chemistry Research 430
:Spring 2017
:Broddie Davis
:Junior Chemistry Major

==Research Times==
M/Tues 1-5 pm
W 12:30-2

: section 02 = 0.50 credit = 8 hours per week.

==Proposed Research Project==
===Enter Project Title here===

===General Information===
:Advisor: Dr. Michael Prinsell
:Other research student collaborators: Amy Wollenburg and Austin Reeder
:Other Research Collaborators:

===Proposal===

===Instruments to be used===

===References (2 minimum)===

===Research pledge===
I, Broddie Davis, have read the Chem/Bioc 430 course syllabus and understand the general structure and expectations of the research program. The above material was prepared after consultation, and in conjunction with my research advisor.

==Written Report==

...from the course syllabus...

[https://www.acs.org/content/dam/acsorg/about/governance/committees/training/acsapproved/degreeprogram/preparing-a-research-report.pdf ACS Guide to Research Reports]

:''Research students are expected to write a report and submit it to the research coordinator by the last day of regular semester classes. These reports are intended to summarize the data collected over the course of the semester. Since this research course requires you to enroll in at least two semesters of research, two reports will be generated. The first semester report should be considered a work in progress, where as the final report should be a more comprehensive summary of your research project. These reports are necessary since several researchers may work on each project. The report will be organized so that it is clear what material is new and what material is review. When available, research students will be provided with an electronic copy of the latest report on their project. The research student is expected to update and improve the introduction, background, and literature sections with each report. Results that challenge earlier conclusions will be justified in a discussion section. Reports will be submitted in both electronic and hard copy to the Faculty Research Advisor AND Research Coordinator.''

===1. Descriptive information===
A project title, the names of the researcher (past and current), faculty research advisor, and other relevant student researchers and/or collaborators, the name and page numbers of the lab notebook(s) where the research is described, the dates when the work was done, and the names of the document file and its immediate precursor.

Example:

'''Detection of Radical Intermediate generated from the MAO enzymatic system.'''

Styles Bitchly*, Donald Hump, Penn Mickey, and Bradley E. Sturgeon#

*lead author, #research advisor

Research work documented in lab notebooks, SB_01 pages 1-25.

===2. Introduction===
State of the motivation for the project of interest in terms of current literature. When we make reference to current literature, this is where you provide specific reference(s) to this work. This section can be largely copied from an earlier report(s), if they exist, but it is expected that this section is edited to include newly found background information. Note: if the author of previous report(s) is included as a contributor to the project, you may cut and paste text; this is not plagiarism, it is collaboration.

===3. Background from earlier reports===
This section will summarize the work reported in earlier reports. If significant results were presented in the most recent report, these results will be summarized and in most cases can be added to that reports background section. This section is included mainly to confirm the current students overall understanding of the project.

===4. Experimental===
This section describes experiments done during the period covered by the report. Usually, this work will be similar or identical to that described in the prior report, if they exists. Any new experiments will be written up and added to the experimental section. Any experiments preformed under identical conditions need only reference previous reports.

:''Example:''

::'''Reagents''': ''List reagents used by product number and the source''.

::'''Enzyme Reactions''': All enzyme reactions were done using a totlal volume of 5.0 mL. Substrate concentration ranged between 1-12 mM. Reactions were initiated be the addition of enzyme.

::'''HPLC''': HPLC data was collected using the Waters Breeze HPLC with a C18 column (insert specs here). Specific HPLC conditions are given in the figure captions.

::'''UV-Vis''': UV-Vis data was collected using the HP 5832 UV-Vis spectrometer using a quartz cuvette. Sample concentrations were adjusted so as to not exceed 1.0 absorbance unit. Significant data was exported in the ".CSV" format and then worked up in Igor.

===5. Results===
This section documents the results of the experiments done during the period covered by the report. Tabulation of data is encouraged; representative spectra presented.

===6. Discussion===
In this section, the student will discuss the results of their work in context of the literature and the results of earlier reports. Questions that have been raised in earlier reports may be addressed here.

===7. Conclusions===
Restate the findings of this period of research. The statement “No conclusions have been reached,” is an acceptable statement.

===8. Future Directions===
In this section, the student will discuss possible experiments intended to address unanswered questions or technical problems on the project.

===9. Literature references===
Literature referenced in the report will be cited. This will be copied from the earlier report, and the student is expected to contribute to the accumulation of relevant literature. Remember that all cited literature must be read.

===10. Signature===
Two copies of the report will be signed and dated and turned in to the Faculty Research Advisor and archived by the Research Coordinator.

Normal and Cold Arm

2016-09-29T01:07:49Z

BroddieD16:

Normal and Cold Arm

:Broddie Davis
:September 22, 2016
:Professor Sturgeon
==Normal Arm==
[[File:ThermalPICture1.jpg]]
Thermal image is of my arm at normal temperature
==Cold Arm==
[[File:ThermalPIcutre2.jpg]]
Thermal image is of my arm at normal temperature

File:ThermalPIcutre2.jpg

2016-09-29T01:06:43Z

BroddieD16:

Normal and Cold Arm

2016-09-29T01:06:23Z

BroddieD16:

Normal and Cold Arm

:Broddie Davis
:September 22, 2016
:Professor Sturgeon
==Normal Arm==
[[File:ThermalPICture1.jpg]]
Thermal image is of my arm at normal temperature
==Cold Arm==
[[File:ThermalPICture2.jpg]]
Thermal image is of my arm at normal temperature

Normal and Cold Arm

2016-09-29T01:04:00Z

BroddieD16: Created page with "Normal and Cold Arm :Broddie Davis :September 22, 2016 :Professor Sturgeon ==Normal Arm== File:ThermalPicture1.jpg Thermal image is of my arm at normal temperature ==Cold..."

Normal and Cold Arm

:Broddie Davis
:September 22, 2016
:Professor Sturgeon
==Normal Arm==
[[File:ThermalPicture1.jpg]]
Thermal image is of my arm at normal temperature
==Cold Arm==
[[File:ThermalPicture2.jpg]]
Thermal image is of my arm at normal temperature

File:ThermalPICture1.jpg

2016-09-29T00:53:52Z

BroddieD16:

Broddie Davis Chem430 F16

2016-09-29T00:41:45Z

BroddieD16:

Chemistry/Biochemistry Research 430
:Fall 2016
:Broddie Davis
:Junior Chemistry Major

==Research Times==
Monday 2pm-6pm

==Proposed Research Project==

Formation of N-N Bonds as a Tool for Synthesis and Drug Development

===General Information===
:Advisor: Michael Prinsell
:Other research student collaborators: Austin Reeder and Amy Wollenburg
:Other Research Collaborators: here

===Proposal===

•Developing a method for creating N-N bonds, using a nucleophilic N and an electrophilic N attached to a leaving group.

===Instruments to be used===
Flash Chromatography, HPLC, GC-MS, H-NMR
===References (2 minimum)===

===Research pledge===
I, Broddie Davis, have read the Chem/Bioc 430 course syllabus and understand the general structure and expectations of the research program. The above material was prepared after consultation, and in conjunction with my research advisor.

Broddie Davis Chem430 F16

2016-09-29T00:41:27Z

BroddieD16:

Chemistry/Biochemistry Research 430
:Fall 2016
:Broddie Davis
:Junior Chemistry Major

==Research Times==
TBD- Monday 2pm-6pm

==Proposed Research Project==

Formation of N-N Bonds as a Tool for Synthesis and Drug Development

===General Information===
:Advisor: Michael Prinsell
:Other research student collaborators: Austin Reeder and Amy Wollenburg
:Other Research Collaborators: here

===Proposal===

•Developing a method for creating N-N bonds, using a nucleophilic N and an electrophilic N attached to a leaving group.

===Instruments to be used===
Flash Chromatography, HPLC, GC-MS, H-NMR
===References (2 minimum)===

===Research pledge===
I, Broddie Davis, have read the Chem/Bioc 430 course syllabus and understand the general structure and expectations of the research program. The above material was prepared after consultation, and in conjunction with my research advisor.

Broddie Davis Chem430 F16

2016-08-26T22:49:34Z

BroddieD16:

Chemistry/Biochemistry Research 430
:Fall 2016
:Broddie Davis
:Junior Chemistry Major

==Research Times==
TBD- 4 hours

==Proposed Research Project==
===Enter Project Title here===

===General Information===
:Advisor: Michael Prinsell
:Other research student collaborators:
:Other Research Collaborators: here

===Proposal===

===Instruments to be used===

===References (2 minimum)===

===Research pledge===
I, Broddie Davis, have read the Chem/Bioc 430 course syllabus and understand the general structure and expectations of the research program. The above material was prepared after consultation, and in conjunction with my research advisor.

Broddie Davis Chem430 F16

2016-08-26T22:44:24Z

BroddieD16: Created page with "Chemistry/Biochemistry Research 430 :Fall 2016 :Broddie Davis :Junior Chemistry Major ==Research Times== ==Proposed Research Project== ===Enter Project Title here=== ===G..."

Chemistry/Biochemistry Research 430
:Fall 2016
:Broddie Davis
:Junior Chemistry Major

==Research Times==

==Proposed Research Project==
===Enter Project Title here===

===General Information===
:Advisor: here
:Other research student collaborators: here
:Other Research Collaborators: here

===Proposal===

===Instruments to be used===

===References (2 minimum)===

===Research pledge===
I, Broddie Davis, have read the Chem/Bioc 430 course syllabus and understand the general structure and expectations of the research program. The above material was prepared after consultation, and in conjunction with my research advisor.